Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7231627
Preview
| Coordinates | 7231627.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H22 Cl0.75 N O3 |
|---|---|
| Calculated formula | C30 H22 Cl0.757 N O3 |
| Title of publication | Advanced palladium free approach to the synthesis of substituted alkene oxindoles via aluminum-promoted Knoevenagel reaction |
| Authors of publication | Novikova, Daria S.; Grigoreva, Tatyana A.; Zolotarev, Andrey A.; Garabadzhiu, Alexander V.; Tribulovich, Vyacheslav G. |
| Journal of publication | RSC Advances |
| Year of publication | 2018 |
| Journal volume | 8 |
| Journal issue | 60 |
| Pages of publication | 34543 |
| a | 10.226 ± 0.0007 Å |
| b | 10.6156 ± 0.0008 Å |
| c | 11.7663 ± 0.0008 Å |
| α | 69.018 ± 0.007° |
| β | 85.368 ± 0.006° |
| γ | 85.951 ± 0.006° |
| Cell volume | 1187.51 ± 0.16 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0553 |
| Residual factor for significantly intense reflections | 0.047 |
| Weighted residual factors for significantly intense reflections | 0.1133 |
| Weighted residual factors for all reflections included in the refinement | 0.1196 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 211386 (current) | 2018-10-11 | cif/ Adding structures of 7231627 via cif-deposit CGI script. |
7231627.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.