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Information card for entry 7238703
Preview
| Coordinates | 7238703.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C19 H30 N2 O9 |
|---|---|
| Calculated formula | C19 H25 N2 O9 |
| Title of publication | Triphenylphosphine-mediated reaction of dialkyl azodicarboxylate with activated alkenes leading to pyrazolines |
| Authors of publication | Yamazaki, Shoko; Maenaka, Yuta; Fujinami, Ken; Mikata, Yuji |
| Journal of publication | RSC Advances |
| Year of publication | 2012 |
| Journal volume | 2 |
| Journal issue | 21 |
| Pages of publication | 8095 |
| a | 9.2138 ± 0.0015 Å |
| b | 9.2556 ± 0.0015 Å |
| c | 14.723 ± 0.003 Å |
| α | 99.6509 ± 0.0016° |
| β | 96.6679 ± 0.0014° |
| γ | 112.748 ± 0.0015° |
| Cell volume | 1118.7 ± 0.3 Å3 |
| Cell temperature | 123 K |
| Ambient diffraction temperature | 123 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for significantly intense reflections | 0.06 |
| Weighted residual factors for all reflections included in the refinement | 0.1697 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.06 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244303 (current) | 2019-11-28 | cif/ Adding structures of 7238703 via cif-deposit CGI script. |
7238703.cif |
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Users of the data should acknowledge the original authors of the
structural data.