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Information card for entry 7239214
Preview
| Coordinates | 7239214.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23 H20 I O6 |
|---|---|
| Calculated formula | C23.004 H20.004 I O6 |
| Title of publication | Hetero Diels‒Alder reaction of olefin with o-quinone methides generated using (±)-binolphosphoric acid for the stereoselective synthesis of 2,4-diarylbenzopyrans: application to the formal synthesis of myristinin B/C |
| Authors of publication | Gharpure, Santosh J.; Sathiyanarayanan, A. M.; Vuram, Prasanna K. |
| Journal of publication | RSC Advances |
| Year of publication | 2013 |
| Journal volume | 3 |
| Journal issue | 40 |
| Pages of publication | 18279 |
| a | 9.333 ± 0.0004 Å |
| b | 9.5986 ± 0.0004 Å |
| c | 14.6529 ± 0.0007 Å |
| α | 107.576 ± 0.002° |
| β | 92.267 ± 0.002° |
| γ | 90.024 ± 0.002° |
| Cell volume | 1250.3 ± 0.1 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0691 |
| Residual factor for significantly intense reflections | 0.06 |
| Weighted residual factors for significantly intense reflections | 0.1982 |
| Weighted residual factors for all reflections included in the refinement | 0.2301 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.025 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244601 (current) | 2019-11-28 | cif/ Adding structures of 7239210, 7239211, 7239212, 7239213, 7239214 via cif-deposit CGI script. |
7239214.cif |
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Users of the data should acknowledge the original authors of the
structural data.