Crystallography Open Database

Information card for entry 7239232

Preview

Coordinates	7239232.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H46 B F3 N O P2 Rh
Calculated formula	C28 H46 B F3 N O P2 Rh
Title of publication	Phosphanyl-substituted π-excess σ2P heterocycles: Coordination behaviour of 2-di-tert-butylphosphanyl-1-neopentyl-1,3-benzazaphosphole towards CuCl, HgCl2 and [Rh(COD)2]BF4
Authors of publication	Ghalib, Mohammed; Jones, Peter G.; Palm, Gottfried J.; Heinicke, Joachim W.
Journal of publication	RSC Advances
Year of publication	2013
Journal volume	3
Journal issue	39
Pages of publication	17726
a	10.70896 ± 0.00015 Å
b	18.337 ± 0.0003 Å
c	14.961 ± 0.0002 Å
α	90°
β	91.102 ± 0.002°
γ	90°
Cell volume	2937.35 ± 0.07 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0389
Residual factor for significantly intense reflections	0.0313
Weighted residual factors for significantly intense reflections	0.0737
Weighted residual factors for all reflections included in the refinement	0.078
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
244609 (current)	2019-11-28	cif/ Adding structures of 7239231, 7239232 via cif-deposit CGI script.	7239232.cif