Crystallography Open Database

Information card for entry 7239804

Preview

Coordinates	7239804.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H73 N3 Si7
Calculated formula	C31 H73 N3 Si7
Title of publication	DMAP-stabilized bis(silyl)silylenes as versatile synthons for organosilicon compounds
Authors of publication	Holzner, Richard; Reiter, Dominik; Frisch, Philipp; Inoue, Shigeyoshi
Journal of publication	RSC Advances
Year of publication	2020
Journal volume	10
Journal issue	6
Pages of publication	3402 - 3406
a	11.515 ± 0.009 Å
b	11.94 ± 0.009 Å
c	16.1 ± 0.007 Å
α	97.728 ± 0.017°
β	92.844 ± 0.018°
γ	104.175 ± 0.019°
Cell volume	2119 ± 2 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0439
Residual factor for significantly intense reflections	0.0402
Weighted residual factors for significantly intense reflections	0.0992
Weighted residual factors for all reflections included in the refinement	0.1016
Goodness-of-fit parameter for all reflections included in the refinement	1.123
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
258055 (current)	2020-10-06	cif/ Updating files of 7239801, 7239802, 7239803, 7239804 Original log message: Adding full bibliography for 7239801--7239804.cif.	7239804.cif
247080	2020-01-22	cif/ Adding structures of 7239801, 7239802, 7239803, 7239804 via cif-deposit CGI script.	7239804.cif