Crystallography Open Database

Information card for entry 7241472

Preview

Coordinates	7241472.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H41 N5 O10 Zn
Calculated formula	C28 H41 N5 O10 Zn
SMILES	N(=O)(=O)[O-].CCO.[Zn]1234([O]=C(N[N]4=Cc4c([OH]1)cccc4)CCCCCO)[O]=C(N[N]3=Cc1c(O2)cccc1)CCCCCO
Title of publication	Effect of N-salicylidene hydrazide protonation on the solid state structural diversity of its Cu(ii), Ni(ii) and Zn(ii) complexes
Authors of publication	Lago, Ana Belén; Pino-Cuevas, Arantxa; Carballo, Rosa; Vázquez-López, Ezequiel M.
Journal of publication	CrystEngComm
Year of publication	2021
Journal volume	23
Journal issue	1
Pages of publication	153 - 162
a	13.6157 ± 0.0014 Å
b	14.5331 ± 0.0016 Å
c	18.1322 ± 0.0019 Å
α	109.291 ± 0.003°
β	110.987 ± 0.003°
γ	95.422 ± 0.003°
Cell volume	3068.3 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1064
Residual factor for significantly intense reflections	0.0901
Weighted residual factors for significantly intense reflections	0.2286
Weighted residual factors for all reflections included in the refinement	0.2389
Goodness-of-fit parameter for all reflections included in the refinement	1.108
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
261592 (current)	2021-02-05	cif/ Updating files of 7241471, 7241472, 7241473, 7241474, 7241475, 7241476 Original log message: Adding full bibliography for 7241471--7241476.cif.	7241472.cif
259293	2020-11-29	cif/ Adding structures of 7241471, 7241472, 7241473, 7241474, 7241475, 7241476 via cif-deposit CGI script.	7241472.cif