Crystallography Open Database

Information card for entry 7241901

7241900 << 7241901 >> 7241902

Preview

Coordinates	7241901.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H28 O11 Os3 P2
Calculated formula	C36 H28 O11 Os3 P2
SMILES	[Os]12([Os]([P](C[P]2(c2ccccc2)c2ccccc2)(c2ccccc2)c2ccccc2)(C#[O])(C#[O])[O]=C([Os]1(C#[O])(C#[O])(C#[O])O)OCC)(C#[O])(C#[O])C#[O]
Title of publication	A new synthetic route for the preparation of [Os3(CO)10(μ-OH)(μ-H)] and its reaction with bis(diphenylphosphino)methane (dppm): syntheses and X-ray structures of two isomers of [Os3(CO)8(μ-OH)(μ-H)(μ-dppm)] and [Os3(CO)7(μ3-CO)(μ3-O)(μ-dppm)]
Authors of publication	Joy, Md. Tuhinur R.; Bhoumik, Nikhil C.; Ghosh, Shishir; Richmond, Michael G.; Kabir, Shariff E.
Journal of publication	RSC Advances
Year of publication	2020
Journal volume	10
Journal issue	73
Pages of publication	44699 - 44711
a	10.9749 ± 0.0008 Å
b	12.9394 ± 0.001 Å
c	14.3221 ± 0.0011 Å
α	74.898 ± 0.004°
β	89.703 ± 0.003°
γ	72.437 ± 0.003°
Cell volume	1866.1 ± 0.3 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0221
Residual factor for significantly intense reflections	0.0176
Weighted residual factors for significantly intense reflections	0.0363
Weighted residual factors for all reflections included in the refinement	0.0377
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
260015 (current)	2020-12-19	cif/ Adding structures of 7241897, 7241898, 7241899, 7241900, 7241901 via cif-deposit CGI script.	7241901.cif