Crystallography Open Database

Information card for entry 7242714

Preview

Coordinates	7242714.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H11 N9 Na2 O4.9 W
Calculated formula	C18 H11 N9 Na2 O4.872 W
Title of publication	Unusual structural changes going from Li+ to Cs+ in [W(CN)6(bpy)]2− ion salts: the Na+ case
Authors of publication	Hodorowicz, Maciej; Jurowska, Anna; Szklarzewicz, Janusz
Journal of publication	CrystEngComm
Year of publication	2021
Journal volume	23
Journal issue	24
Pages of publication	4301 - 4311
a	8.5595 ± 0.0002 Å
b	9.8622 ± 0.0001 Å
c	13.8861 ± 0.0003 Å
α	94.349 ± 0.001°
β	99.66 ± 0.002°
γ	98.206 ± 0.001°
Cell volume	1137.75 ± 0.04 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0542
Residual factor for significantly intense reflections	0.0469
Weighted residual factors for significantly intense reflections	0.1191
Weighted residual factors for all reflections included in the refinement	0.1232
Goodness-of-fit parameter for all reflections included in the refinement	1.076
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
267099 (current)	2021-07-05	cif/ Updating files of 7242713, 7242714 Original log message: Adding full bibliography for 7242713--7242714.cif.	7242714.cif
264508	2021-04-25	cif/ Adding structures of 7242713, 7242714 via cif-deposit CGI script.	7242714.cif