Crystallography Open Database

Information card for entry 7245770

Preview

Coordinates	7245770.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C115 H165 Dy4 N45 O29
Calculated formula	C115 H163 Dy4 N45 O28
Title of publication	Syntheses, structures and magnetic properties of mononuclear, dinuclear and tetranuclear dysprosium(III) complexes based on azotetrazole-3-hydroxy-2-naphthoic acid
Authors of publication	Zhong, Yun-Jing; Zhu, Yu-Ying; Mo, Jin-Lin; Ye, Sheng-Lan; Luo, Wen-Dan; Huang, Xin; Chen, Wen-Bin; Dong, Wen
Journal of publication	CrystEngComm
Year of publication	2022
a	14.5277 ± 0.0002 Å
b	19.59 ± 0.0003 Å
c	24.9631 ± 0.0004 Å
α	85.482 ± 0.001°
β	76.15 ± 0.001°
γ	75.698 ± 0.001°
Cell volume	6682.64 ± 0.18 Å³
Cell temperature	99.99 ± 0.1 K
Ambient diffraction temperature	99.99 ± 0.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0877
Residual factor for significantly intense reflections	0.0707
Weighted residual factors for significantly intense reflections	0.1549
Weighted residual factors for all reflections included in the refinement	0.1635
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
279042 (current)	2022-11-08	cif/ Adding structures of 7245767, 7245768, 7245769, 7245770 via cif-deposit CGI script.	7245770.cif