Crystallography Open Database

Information card for entry 7248436

Preview

Coordinates	7248436.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C11 H9 N9 O Pb
Calculated formula	C11 H9 N9 O Pb
Title of publication	Structural diversity and tetrel bonding significance in lead(ii) complexes with pyrazoylisonicotinoylhydrazone and varied anionic co-ligands
Authors of publication	Mahmoudi, Ghodrat; García-Santos, Isabel; Fernández-Vázquez, Roi; Gomila, Rosa M.; Castiñeiras, Alfonso; Doustkhah, Esmail; Zangrando, Ennio; Frontera, Antonio
Journal of publication	CrystEngComm
Year of publication	2024
Journal volume	26
Journal issue	19
Pages of publication	2526 - 2535
a	8.7307 ± 0.0003 Å
b	16.6328 ± 0.0007 Å
c	9.6082 ± 0.0004 Å
α	90°
β	100.146 ± 0.001°
γ	90°
Cell volume	1373.45 ± 0.09 Å³
Cell temperature	250 ± 2 K
Ambient diffraction temperature	250 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0175
Residual factor for significantly intense reflections	0.0144
Weighted residual factors for significantly intense reflections	0.0303
Weighted residual factors for all reflections included in the refinement	0.0311
Goodness-of-fit parameter for all reflections included in the refinement	1.09
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
292956 (current)	2024-07-05	cif/ Updating files of 7248436, 7248437, 7248438, 7248439 Original log message: Adding full bibliography for 7248436--7248439.cif.	7248436.cif
291262	2024-04-18	cif/ Adding structures of 7248436, 7248437, 7248438, 7248439 via cif-deposit CGI script.	7248436.cif