Crystallography Open Database

Information card for entry 7700965

Preview

Coordinates	7700965.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34.1 H26 O0.1 Si2
Calculated formula	C34.103 H26 O0.103 Si2
Title of publication	Synthesis, characterisation and electronic properties of naphthalene bridged disilanes.
Authors of publication	Rabanzo-Castillo, Kristel M; Hanif, Muhammad; Söhnel, Tilo; Leitao, Erin M.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	37
Pages of publication	13971 - 13980
a	15.6489 ± 0.0003 Å
b	8.8195 ± 0.0001 Å
c	19.3548 ± 0.0003 Å
α	90°
β	106.959 ± 0.002°
γ	90°
Cell volume	2555.1 ± 0.07 Å³
Cell temperature	110 ± 1 K
Ambient diffraction temperature	110 ± 1 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0354
Residual factor for significantly intense reflections	0.0326
Weighted residual factors for significantly intense reflections	0.0892
Weighted residual factors for all reflections included in the refinement	0.0914
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
223851 (current)	2019-11-07	cif/ Updating files of 7700964, 7700965, 7700966, 7700967, 7700968, 7700969 Original log message: Adding full bibliography for 7700964--7700969.cif.	7700965.cif
217855	2019-08-30	cif/ Adding structures of 7700964, 7700965, 7700966, 7700967, 7700968, 7700969 via cif-deposit CGI script.	7700965.cif