Crystallography Open Database

Information card for entry 7702855

Preview

Coordinates	7702855.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H40 Ga2 I2 N4
Calculated formula	C20 H40 Ga2 I2 N4
Title of publication	The reactivity of diazabutadienes toward low oxidation state Group 13 iodides and the synthesis of a new gallium(i) carbene analogue
Authors of publication	Baker, Robert J.; Farley, Robert D.; Jones, Cameron; Kloth, Marc; Murphy, Damien M.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	20
Pages of publication	3844
a	10.733 ± 0.0015 Å
b	10.733 ± 0.0015 Å
c	24.88 ± 0.005 Å
α	90°
β	90°
γ	90°
Cell volume	2866.1 ± 0.8 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	92
Hermann-Mauguin space group symbol	P 41 21 2
Hall space group symbol	P 4abw 2nw
Residual factor for all reflections	0.0258
Residual factor for significantly intense reflections	0.0239
Weighted residual factors for significantly intense reflections	0.0517
Weighted residual factors for all reflections included in the refinement	0.0524
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
244051 (current)	2019-11-28	cif/ Adding structures of 7702853, 7702854, 7702855, 7702856, 7702857, 7702858, 7702859 via cif-deposit CGI script.	7702855.cif