Crystallography Open Database

Information card for entry 7703163

Preview

Coordinates	7703163.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H29 N3 P2
Calculated formula	C38 H29 N3 P2
Title of publication	New 1,2,3-triazole based bis- and trisphosphine ligands: synthesis, transition metal chemistry and catalytic studies.
Authors of publication	Radhakrishna, Latchupatula; Kunchur, Harish S.; Namdeo, Pavan K.; Butcher, Ray J.; Balakrishna, Maravanji S.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	11
Pages of publication	3434 - 3449
a	11.9846 ± 0.0004 Å
b	17.046 ± 0.0006 Å
c	17.7261 ± 0.0005 Å
α	111.601 ± 0.003°
β	93.453 ± 0.003°
γ	110.334 ± 0.003°
Cell volume	3082.7 ± 0.2 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1433
Residual factor for significantly intense reflections	0.0773
Weighted residual factors for significantly intense reflections	0.1793
Weighted residual factors for all reflections included in the refinement	0.232
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
250303 (current)	2020-04-05	cif/ Updating files of 7703162, 7703163, 7703164, 7703165, 7703166, 7703167, 7703168, 7703169, 7703170, 7703171, 7703172 Original log message: Adding full bibliography for 7703162--7703172.cif.	7703163.cif
246465	2020-01-03	cif/ Adding structures of 7703162, 7703163, 7703164, 7703165, 7703166, 7703167, 7703168, 7703169, 7703170, 7703171, 7703172 via cif-deposit CGI script.	7703163.cif