Crystallography Open Database

Information card for entry 7703262

Preview

Coordinates	7703262.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H30 B F20 Sb
Calculated formula	C44 H30 B F20 Sb
Title of publication	Diverse structure and reactivity of pentamethylcyclopentadienyl antimony(iii) cations.
Authors of publication	Coughlin, Omar; Krämer, Tobias; Benjamin, Sophie L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	6
Pages of publication	1726 - 1730
a	12.4426 ± 0.0004 Å
b	12.7883 ± 0.0004 Å
c	15.2203 ± 0.0005 Å
α	108.476 ± 0.003°
β	104.868 ± 0.003°
γ	103.354 ± 0.003°
Cell volume	2087.32 ± 0.14 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0714
Residual factor for significantly intense reflections	0.0452
Weighted residual factors for significantly intense reflections	0.0853
Weighted residual factors for all reflections included in the refinement	0.0978
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
248949 (current)	2020-03-05	cif/ Updating files of 7703262, 7703263, 7703264, 7703265, 7703266, 7703267 Original log message: Adding full bibliography for 7703262--7703267.cif.	7703262.cif
246796	2020-01-14	cif/ Adding structures of 7703262, 7703263, 7703264, 7703265, 7703266, 7703267 via cif-deposit CGI script.	7703262.cif