Crystallography Open Database

Information card for entry 7703339

Preview

Coordinates	7703339.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	P(N3)-P=N
Formula	C54 H45 Cl3 N4 O2 P2 U
Calculated formula	C54 H45 Cl3 N4 O2 P2 U
Title of publication	Consecutive N<sub>2</sub> loss from a uranium diphosphazide complex.
Authors of publication	Dickie, Tara K. K.; MacNeil, Connor S.; Hayes, Paul G.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	3
Pages of publication	578 - 582
a	13.7944 ± 0.0001 Å
b	17.44271 ± 0.00012 Å
c	20.4207 ± 0.00016 Å
α	90°
β	94.9425 ± 0.0007°
γ	90°
Cell volume	4895.19 ± 0.06 Å³
Cell temperature	100 ± 0.13 K
Ambient diffraction temperature	100 ± 0.13 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0301
Residual factor for significantly intense reflections	0.0291
Weighted residual factors for significantly intense reflections	0.0792
Weighted residual factors for all reflections included in the refinement	0.08
Goodness-of-fit parameter for all reflections included in the refinement	1.124
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
247074 (current)	2020-01-22	cif/ Adding structures of 7703336, 7703337, 7703338, 7703339, 7703340 via cif-deposit CGI script.	7703339.cif