Crystallography Open Database

Information card for entry 7703377

Preview

Coordinates	7703377.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C4 H10 Cl3 S3 W
Calculated formula	C4 H10 Cl3 S3 W
Title of publication	Thioether complexes of WSCl<sub>4</sub>, WOCl<sub>4</sub> and WSCl<sub>3</sub> and evaluation of thiochloride complexes as CVD precursors for WS<sub>2</sub> thin films.
Authors of publication	Smith, Danielle E.; Greenacre, Victoria K.; Hector, Andrew L.; Huang, Ruomeng; Levason, William; Reid, Gillian; Robinson, Fred; Thomas, Shibin
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	8
Pages of publication	2496 - 2504
a	6.8758 ± 0.0001 Å
b	13.2588 ± 0.0002 Å
c	12.5782 ± 0.0002 Å
α	90°
β	94.541 ± 0.002°
γ	90°
Cell volume	1143.09 ± 0.03 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0432
Residual factor for significantly intense reflections	0.0391
Weighted residual factors for significantly intense reflections	0.0748
Weighted residual factors for all reflections included in the refinement	0.0763
Goodness-of-fit parameter for all reflections included in the refinement	1.085
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
248909 (current)	2020-03-05	cif/ Updating files of 7703371, 7703372, 7703373, 7703374, 7703375, 7703376, 7703377 Original log message: Adding full bibliography for 7703371--7703377.cif.	7703377.cif
247332	2020-01-29	cif/ Adding structures of 7703371, 7703372, 7703373, 7703374, 7703375, 7703376, 7703377 via cif-deposit CGI script.	7703377.cif