Crystallography Open Database

Information card for entry 7703421

Preview

Coordinates	7703421.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H42 Cl4 Co2 N10 O18
Calculated formula	C40 H42 Cl4 Co2 N10 O18
Title of publication	Oxidative C-N bond cleavage of (2-pyridylmethyl)amine-based tetradentate supporting ligands in ternary cobalt(ii)-carboxylate complexes.
Authors of publication	Chakraborty, Biswarup; Ghosh, Ivy; Jana, Rahul Dev; Paine, Tapan Kanti
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	11
Pages of publication	3463 - 3472
a	16.4332 ± 0.0017 Å
b	18.9379 ± 0.0019 Å
c	18.6337 ± 0.0019 Å
α	90°
β	113.438 ± 0.001°
γ	90°
Cell volume	5320.5 ± 0.9 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.071
Residual factor for significantly intense reflections	0.0561
Weighted residual factors for significantly intense reflections	0.1106
Weighted residual factors for all reflections included in the refinement	0.1152
Goodness-of-fit parameter for all reflections included in the refinement	1.266
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
250301 (current)	2020-04-05	cif/ Updating files of 7703417, 7703418, 7703419, 7703420, 7703421 Original log message: Adding full bibliography for 7703417--7703421.cif.	7703421.cif
247428	2020-02-01	cif/ Adding structures of 7703417, 7703418, 7703419, 7703420, 7703421 via cif-deposit CGI script.	7703421.cif