Crystallography Open Database

Information card for entry 7703445

Preview

Coordinates	7703445.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H38 Cl2 N6 O4 Pd
Calculated formula	C28 H38 Cl2 N6 O4 Pd
Title of publication	Brønsted and Lewis acid adducts of triazenes.
Authors of publication	Landman, Iris R.; Suleymanov, Abdusalom A.; Fadaei-Tirani, Farzaneh; Scopelliti, Rosario; Chadwick, F. Mark; Severin, Kay
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	7
Pages of publication	2317 - 2322
a	8.1628 ± 0.0004 Å
b	8.4628 ± 0.0004 Å
c	12.1951 ± 0.0006 Å
α	98.576 ± 0.004°
β	106.738 ± 0.004°
γ	90.52 ± 0.004°
Cell volume	796.52 ± 0.07 Å³
Cell temperature	150.01 ± 0.1 K
Ambient diffraction temperature	150.01 ± 0.1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0365
Residual factor for significantly intense reflections	0.0354
Weighted residual factors for significantly intense reflections	0.0926
Weighted residual factors for all reflections included in the refinement	0.0937
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
248969 (current)	2020-03-05	cif/ Updating files of 7703444, 7703445, 7703446, 7703447, 7703448, 7703449, 7703450 Original log message: Adding full bibliography for 7703444--7703450.cif.	7703445.cif
247879	2020-02-05	cif/ Adding structures of 7703444, 7703445, 7703446, 7703447, 7703448, 7703449, 7703450 via cif-deposit CGI script.	7703445.cif