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Information card for entry 7703752
Preview
| Coordinates | 7703752.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C35 H42 Cl F6 Fe N3 P Pd Sb |
|---|---|
| Calculated formula | C35 H42 Cl F6 Fe N3 P Pd Sb |
| SMILES | [Pd]12(Cl)[Fe]3456789%10([c]%11([P]1(c1ccccc1)c1ccccc1)[cH]4[cH]5[cH]6[cH]7%11)[c]1([cH]8[cH]9[cH]%10[cH]31)[N]2=C(NC1CCCCC1)NC1CCCCC1.[Sb](F)(F)(F)(F)(F)[F-] |
| Title of publication | Synthesis and study of Fe →Pd interactions in unsymmetric Pd(ii) complexes with phosphinoferrocene guanidine ligands. |
| Authors of publication | Bárta, Ondřej; Gyepes, Róbert; Císařová, Ivana; Alemayehu, Adam; Štěpnička, Petr |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2020 |
| Journal volume | 49 |
| Journal issue | 14 |
| Pages of publication | 4225 - 4229 |
| a | 10.5019 ± 0.0006 Å |
| b | 10.3649 ± 0.0006 Å |
| c | 17.149 ± 0.0009 Å |
| α | 90° |
| β | 103.169 ± 0.002° |
| γ | 90° |
| Cell volume | 1817.6 ± 0.18 Å3 |
| Cell temperature | 120 ± 2 K |
| Ambient diffraction temperature | 120 ± 2 K |
| Number of distinct elements | 9 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0126 |
| Residual factor for significantly intense reflections | 0.0124 |
| Weighted residual factors for significantly intense reflections | 0.0312 |
| Weighted residual factors for all reflections included in the refinement | 0.0317 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 251644 (current) | 2020-05-05 | cif/ Updating files of 7703751, 7703752, 7703753, 7703754, 7703755, 7703756, 7703757 Original log message: Adding full bibliography for 7703751--7703757.cif. |
7703752.cif |
| 249429 | 2020-03-17 | cif/ Adding structures of 7703751, 7703752, 7703753, 7703754, 7703755, 7703756, 7703757 via cif-deposit CGI script. |
7703752.cif |
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Users of the data should acknowledge the original authors of the
structural data.