Crystallography Open Database

Information card for entry 7704147

Preview

Coordinates	7704147.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C13 H32 Cl N3 Si2 Sn
Calculated formula	C13 H32 Cl0.9996 N3 Si2 Sn0.9996
Title of publication	Synthesis and characterization of guanidinate tin(ii) complexes for ring-opening polymerization of cyclic esters.
Authors of publication	Ungpittagul, Thasanaporn; Wongmahasirikun, Phonpimon; Phomphrai, Khamphee
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	25
Pages of publication	8460 - 8471
a	9.0266 ± 0.0005 Å
b	15.8031 ± 0.001 Å
c	15.9397 ± 0.001 Å
α	67.3 ± 0.002°
β	83.976 ± 0.002°
γ	83.677 ± 0.002°
Cell volume	2080 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0647
Residual factor for significantly intense reflections	0.0402
Weighted residual factors for significantly intense reflections	0.0721
Weighted residual factors for all reflections included in the refinement	0.0779
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
253899 (current)	2020-07-06	cif/ Updating files of 7704145, 7704146, 7704147, 7704148 Original log message: Adding full bibliography for 7704145--7704148.cif.	7704147.cif
250999	2020-04-22	cif/ Adding structures of 7704145, 7704146, 7704147, 7704148 via cif-deposit CGI script.	7704147.cif