Crystallography Open Database

Information card for entry 7705571

Preview

Coordinates	7705571.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H42 F36 K2 O16 Sn
Calculated formula	C39 H42 F36 K2 O16 Sn
Title of publication	Formation of monomeric Sn(ii) and Sn(iv) perfluoropinacolate complexes and their characterization by <sup>119</sup>Sn Mössbauer and <sup>119</sup>Sn NMR spectroscopies.
Authors of publication	Elinburg, Jessica K.; Hyre, Ariel S.; McNeely, James; Alam, Todd M.; Klenner, Steffen; Pöttgen, Rainer; Rheingold, Arnold L.; Doerrer, Linda H.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	39
Pages of publication	13773 - 13785
a	15.1378 ± 0.0016 Å
b	16.2438 ± 0.0016 Å
c	16.2454 ± 0.0016 Å
α	99.54 ± 0.003°
β	114.932 ± 0.003°
γ	112.822 ± 0.003°
Cell volume	3068.9 ± 0.6 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0488
Residual factor for significantly intense reflections	0.0402
Weighted residual factors for significantly intense reflections	0.1045
Weighted residual factors for all reflections included in the refinement	0.1102
Goodness-of-fit parameter for all reflections included in the refinement	1.127
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
258825 (current)	2020-11-06	cif/ Updating files of 7705569, 7705570, 7705571, 7705572, 7705573 Original log message: Adding full bibliography for 7705569--7705573.cif.	7705571.cif
256910	2020-10-02	cif/ Adding structures of 7705569, 7705570, 7705571, 7705572, 7705573 via cif-deposit CGI script.	7705571.cif