Crystallography Open Database

Information card for entry 7705893

Preview

Coordinates	7705893.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Dy3 K4 Na4.75 O138.33 Sb3 W31
Calculated formula	Dy3 K4 Na4.75 O138.333 Sb4 W30
Title of publication	Ionic strength effect on regulating the synthetic assembly of polyoxometalate clusters with slow magnetic relaxation behavior.
Authors of publication	Cai, Jing; Ye, Run; Liu, Xinhao; Guo, Leilei; Qiao, Xinrong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	46
Pages of publication	16954 - 16961
a	35.159 ± 0.003 Å
b	18.5597 ± 0.0007 Å
c	48.357 ± 0.003 Å
α	90°
β	114.193 ± 0.009°
γ	90°
Cell volume	28783 ± 4 Å³
Cell temperature	191 ± 2 K
Ambient diffraction temperature	191 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1583
Residual factor for significantly intense reflections	0.1059
Weighted residual factors for significantly intense reflections	0.2022
Weighted residual factors for all reflections included in the refinement	0.2298
Goodness-of-fit parameter for all reflections included in the refinement	1.086
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
259698 (current)	2020-12-09	cif/ Adding structures of 7705891, 7705892, 7705893 via cif-deposit CGI script.	7705893.cif