Crystallography Open Database

Information card for entry 7706443

Preview

Coordinates	7706443.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H29 Cl3 Ge2
Calculated formula	C17 H29 Cl3 Ge2
Title of publication	Pentamethyl- and 1,2,4-tri(tert-butyl)cyclopentadienyl containing p-block complexes - differences and similarities.
Authors of publication	Ding, Yi; Ruth, Paul Niklas; Herbst-Irmer, Regine; Stalke, Dietmar; Yang, Zhi; Roesky, Herbert W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	6
Pages of publication	2067 - 2074
a	17.206 ± 0.002 Å
b	9.715 ± 0.002 Å
c	25.399 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	4245.6 ± 1.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0299
Residual factor for significantly intense reflections	0.0271
Weighted residual factors for significantly intense reflections	0.0614
Weighted residual factors for all reflections included in the refinement	0.0622
Goodness-of-fit parameter for all reflections included in the refinement	1.232
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
262630 (current)	2021-03-05	cif/ Updating files of 7706437, 7706438, 7706439, 7706440, 7706441, 7706442, 7706443 Original log message: Adding full bibliography for 7706437--7706443.cif.	7706443.cif
261069	2021-01-20	cif/ Adding structures of 7706437, 7706438, 7706439, 7706440, 7706441, 7706442, 7706443 via cif-deposit CGI script.	7706443.cif