Crystallography Open Database

Information card for entry 7707095

Preview

Coordinates	7707095.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H61.5 Bi K6.17 N4 O96.67 P2 W22
Calculated formula	C16 H48 Bi K6.16667 N4 O96.6666 P2 W22
Title of publication	Keggin-type polyoxometalate 1 : 1 complexes of Pb(II) and Bi(III): experimental, theoretical and luminescence studies.
Authors of publication	Mukhacheva, Anna A.; Asanova, Tatiana; Ryzhikov, Maxim R.; Sukhikh, Taisiya S.; Kompankov, Nikolay B.; Yanshole, Vadim V.; Berezin, Alexey S.; Gushchin, Artem L.; Abramov, Pavel A.; Sokolov, Maxim N.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	20
Pages of publication	6913 - 6922
a	48.525 ± 0.003 Å
b	12.692 ± 0.0008 Å
c	56.67 ± 0.003 Å
α	90°
β	109.593 ± 0.002°
γ	90°
Cell volume	32881 ± 3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0994
Residual factor for significantly intense reflections	0.0722
Weighted residual factors for significantly intense reflections	0.1297
Weighted residual factors for all reflections included in the refinement	0.139
Goodness-of-fit parameter for all reflections included in the refinement	1.131
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
266042 (current)	2021-06-05	cif/ Updating files of 7707095 Original log message: Adding full bibliography for 7707095.cif.	7707095.cif
264108	2021-04-14	cif/ Adding structures of 7707095 via cif-deposit CGI script.	7707095.cif