Crystallography Open Database

Information card for entry 7707132

Preview

Coordinates	7707132.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	beta 4THF Mg(SCN)
Formula	C18 H32 Mg N2 O4 S2
Calculated formula	C18 Mg N2 O4 S2
Title of publication	Synthesis, characterization and thermal behaviour of solid phases in the quasi-ternary system Mg(SCN)<sub>2</sub>-H<sub>2</sub>O-THF.
Authors of publication	Joos, Markus; Conrad, Maurice; Merkle, Rotraut; Schleid, Thomas; Maier, Joachim; Dinnebier, Robert E.; Bette, Sebastian
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	20
Pages of publication	6949 - 6961
a	10.5624 ± 0.0004 Å
b	15.0999 ± 0.0005 Å
c	7.8918 ± 0.0002 Å
α	90°
β	96.5777 ± 0.0014°
γ	90°
Cell volume	1250.39 ± 0.07 Å³
Cell temperature	433 K
Ambient diffraction temperature	433 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/a 1
Hall space group symbol	-P 2yab
RFsqd	0.0359
Method of determination	powder diffraction
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.5406 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
266033 (current)	2021-06-05	cif/ Updating files of 7707128, 7707129, 7707130, 7707131, 7707132 Original log message: Adding full bibliography for 7707128--7707132.cif.	7707132.cif
264231	2021-04-16	cif/ Adding structures of 7707128, 7707129, 7707130, 7707131, 7707132 via cif-deposit CGI script.	7707132.cif