Crystallography Open Database

Information card for entry 7707836

Preview

Coordinates	7707836.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H84 Co4 Ge O12 P4
Calculated formula	C48 H84 Co4 Ge O12 P4
Title of publication	GeCl<sub>x</sub>[Co(CO)<sub>3</sub>PR<sub>3</sub>]<sub>4-x</sub> (x = 0-3; R = <sup>n</sup>Pr, <sup>n</sup>Bu): from cobalt substituted germanes to novel binary cluster compounds.
Authors of publication	Preißing, Lars; Behling, Elias; Schnepf, Andreas
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	31
Pages of publication	10789 - 10797
a	28.9936 ± 0.0006 Å
b	28.9936 ± 0.0006 Å
c	28.9936 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	24372.9 ± 0.9 Å³
Cell temperature	150 K
Ambient diffraction temperature	150.01 K
Number of distinct elements	6
Space group number	198
Hermann-Mauguin space group symbol	P 21 3
Hall space group symbol	P 2ac 2ab 3
Residual factor for all reflections	0.0831
Residual factor for significantly intense reflections	0.0529
Weighted residual factors for significantly intense reflections	0.1214
Weighted residual factors for all reflections included in the refinement	0.137
Goodness-of-fit parameter for all reflections included in the refinement	1.024
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
268792 (current)	2021-09-06	cif/ Updating files of 7707835, 7707836, 7707837, 7707838, 7707839, 7707840, 7707841 Original log message: Adding full bibliography for 7707835--7707841.cif.	7707836.cif
267576	2021-07-16	cif/ Adding structures of 7707835, 7707836, 7707837, 7707838, 7707839, 7707840, 7707841 via cif-deposit CGI script.	7707836.cif