Crystallography Open Database

Information card for entry 7708091

Preview

Coordinates	7708091.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H58 Cl2 Ga N3
Calculated formula	C46 H58 Cl2 Ga N3
Title of publication	A bis(imino)carbazolate pincer ligand stabilized mononuclear gallium(I) compound: synthesis, characterization, and reactivity.
Authors of publication	Li, Hao; He, Yuhao; Liu, Chunmeng; Tan, Gengwen
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	36
Pages of publication	12674 - 12680
a	12.5642 ± 0.001 Å
b	14.3473 ± 0.0012 Å
c	23.322 ± 0.002 Å
α	90°
β	100.111 ± 0.002°
γ	90°
Cell volume	4138.8 ± 0.6 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.08
Residual factor for significantly intense reflections	0.0553
Weighted residual factors for significantly intense reflections	0.1372
Weighted residual factors for all reflections included in the refinement	0.1574
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
269724 (current)	2021-10-06	cif/ Updating files of 7708091, 7708092, 7708093, 7708094, 7708095, 7708096, 7708097 Original log message: Adding full bibliography for 7708091--7708097.cif.	7708091.cif
268146	2021-08-20	cif/ Adding structures of 7708091, 7708092, 7708093, 7708094, 7708095, 7708096, 7708097 via cif-deposit CGI script.	7708091.cif