Crystallography Open Database

Information card for entry 7708918

Preview

Coordinates	7708918.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H30 As2 Cl2 Pd
Calculated formula	C36 H30 As2 Cl2 Pd
Title of publication	Tertiary arsine ligands for the Stille coupling reaction.
Authors of publication	Chishiro, Akane; Konishi, Masafumi; Inaba, Ryoto; Yumura, Takashi; Imoto, Hiroaki; Naka, Kensuke
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	51
Journal issue	1
Pages of publication	95 - 103
a	15.146 ± 0.0014 Å
b	20.0852 ± 0.0019 Å
c	10.5283 ± 0.001 Å
α	90°
β	92.131 ± 0.009°
γ	90°
Cell volume	3200.6 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1388
Residual factor for significantly intense reflections	0.058
Weighted residual factors for significantly intense reflections	0.0987
Weighted residual factors for all reflections included in the refinement	0.1249
Goodness-of-fit parameter for all reflections included in the refinement	0.987
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272648 (current)	2022-02-04	cif/ Updating files of 7708916, 7708917, 7708918, 7708919, 7708920 Original log message: Adding full bibliography for 7708916--7708920.cif.	7708918.cif
270869	2021-11-25	cif/ Adding structures of 7708916, 7708917, 7708918, 7708919, 7708920 via cif-deposit CGI script.	7708918.cif