Crystallography Open Database

Information card for entry 7709296

Preview

Coordinates	7709296.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C71.5 H62 Cl F12 P4 Pd4
Calculated formula	C71.5 H62 Cl F12 P4 Pd4
Title of publication	Bridging coordination of acenaphthylene to a Pd<sub>3</sub> chain or a Pd<sub>4</sub> sheet cluster.
Authors of publication	Yamamoto, Koji; Sugawa, Tsuyoshi; Kondo, Mio; Masaoka, Shigeyuki; Murahashi, Tetsuro
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2022
Journal volume	51
Journal issue	5
Pages of publication	1901 - 1906
a	10.7362 ± 0.0004 Å
b	18.4776 ± 0.0006 Å
c	19.2924 ± 0.0006 Å
α	115.372 ± 0.0009°
β	97.035 ± 0.0012°
γ	90.4714 ± 0.0012°
Cell volume	3424.2 ± 0.2 Å³
Cell temperature	165 K
Ambient diffraction temperature	165 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0823
Residual factor for significantly intense reflections	0.0668
Weighted residual factors for significantly intense reflections	0.1996
Weighted residual factors for all reflections included in the refinement	0.2125
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
272671 (current)	2022-02-04	cif/ Updating files of 7709295, 7709296 Original log message: Adding full bibliography for 7709295--7709296.cif.	7709296.cif
272013	2022-01-13	cif/ Adding structures of 7709295, 7709296 via cif-deposit CGI script.	7709296.cif