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Information card for entry 7711861
Preview
| Coordinates | 7711861.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H60 N4 Sb2 Si2 |
|---|---|
| Calculated formula | C32 H60 N4 Sb2 Si2 |
| Title of publication | The reactivity of antimony and bismuth <i>N</i>,<i>C</i>,<i>N</i>-pincer compounds toward K[BEt<sub>3</sub>H] - the formation of heterocyclic compounds <i>vs</i>. element-element bonds <i>vs.</i> stable terminal Sb-H bonds. |
| Authors of publication | Novák, Pavel; Erben, Milan; Jambor, Roman; Hejda, Martin; Růžička, Aleš; Rychagova, Elena; Ketkov, Sergey; Dostál, Libor |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2022 |
| Journal volume | 52 |
| Journal issue | 1 |
| Pages of publication | 218 - 227 |
| a | 9.6926 ± 0.0005 Å |
| b | 9.9028 ± 0.0006 Å |
| c | 11.5941 ± 0.0007 Å |
| α | 114.372 ± 0.002° |
| β | 101.681 ± 0.002° |
| γ | 96.559 ± 0.002° |
| Cell volume | 967.98 ± 0.1 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0233 |
| Residual factor for significantly intense reflections | 0.0219 |
| Weighted residual factors for significantly intense reflections | 0.052 |
| Weighted residual factors for all reflections included in the refinement | 0.0533 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.144 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 283232 (current) | 2023-05-05 | cif/ Updating files of 7711860, 7711861, 7711862, 7711863, 7711864, 7711865 Original log message: Adding full bibliography for 7711860--7711865.cif. |
7711861.cif |
| 279661 | 2022-12-01 | cif/ Adding structures of 7711860, 7711861, 7711862, 7711863, 7711864, 7711865 via cif-deposit CGI script. |
7711861.cif |
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Users of the data should acknowledge the original authors of the
structural data.