Crystallography Open Database

Information card for entry 7712216

Preview

Coordinates	7712216.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C105.5 H64 B2 Cl F48 P3 Sn
Calculated formula	C105.5 H64 B2 Cl F48 P3 Sn
Title of publication	Synthesis, spectroscopic and structural properties of Sn(II) and Pb(II) triflate complexes with soft phosphine and arsine coordination.
Authors of publication	Cairns, Kelsey R.; King, Rhys P.; Bannister, Robert D.; Levason, William; Reid, Gillian
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	52
Journal issue	8
Pages of publication	2293 - 2308
a	12.7643 ± 0.0002 Å
b	16.7092 ± 0.0002 Å
c	26.6628 ± 0.0003 Å
α	78.501 ± 0.001°
β	89.422 ± 0.001°
γ	69.688 ± 0.001°
Cell volume	5215.19 ± 0.13 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100.15 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0536
Residual factor for significantly intense reflections	0.0443
Weighted residual factors for significantly intense reflections	0.0987
Weighted residual factors for all reflections included in the refinement	0.1032
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283245 (current)	2023-05-05	cif/ Updating files of 7712208, 7712209, 7712210, 7712211, 7712212, 7712213, 7712214, 7712215, 7712216, 7712217, 7712218, 7712219 Original log message: Adding full bibliography for 7712208--7712219.cif.	7712216.cif
280681	2023-01-31	cif/ Adding structures of 7712208, 7712209, 7712210, 7712211, 7712212, 7712213, 7712214, 7712215, 7712216, 7712217, 7712218, 7712219 via cif-deposit CGI script.	7712216.cif