Crystallography Open Database

Information card for entry 7713224

Preview

Coordinates	7713224.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[Lu2(C4O4)3(H2O)8]n
Chemical name	lutetium(III) squarate
Formula	C12 H16 Lu2 O20
Calculated formula	C12 H16 Lu2 O20
Title of publication	Bilayered lanthanide squarate hydrates (Ln = Eu to Lu) and magnetization reversal barriers of 21 K for Ln = Tm and 57 K for Yb.
Authors of publication	Takano, Rina; Masuda, Koki; Cho, Keigo; Kitagawa, Yasutaka; Ishida, Takayuki
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
a	11.9151 ± 0.0005 Å
b	8.1066 ± 0.0003 Å
c	9.9577 ± 0.0004 Å
α	90°
β	95.748 ± 0.004°
γ	90°
Cell volume	956.99 ± 0.07 Å³
Cell temperature	297.95 ± 0.1 K
Ambient diffraction temperature	297.95 ± 0.1 K
Number of distinct elements	4
Space group number	7
Hermann-Mauguin space group symbol	P 1 c 1
Hall space group symbol	P -2yc
Residual factor for all reflections	0.034
Residual factor for significantly intense reflections	0.0281
Weighted residual factors for significantly intense reflections	0.0793
Weighted residual factors for all reflections included in the refinement	0.0847
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
284139 (current)	2023-06-02	cif/ Adding structures of 7713218, 7713219, 7713220, 7713221, 7713222, 7713223, 7713224, 7713225 via cif-deposit CGI script.	7713224.cif