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Information card for entry 7714276
Preview
| Coordinates | 7714276.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C44 H74 N2 Ru2 |
|---|---|
| Calculated formula | C44 H66 N2 Ru2 |
| Title of publication | Synthesis of Diruthenium μ-η4-α-Diimine Complex via Dehydrogenative Coupling of Cyclic Amines and Its Role in Dehydrogenative Oxidation of Pyrrolidine |
| Authors of publication | Takao, Toshihiro; Shimogawa, Ryuichi; Fujita, Ryosuke; Egawa, Shu |
| Journal of publication | Dalton Transactions |
| Year of publication | 2023 |
| a | 16.9579 ± 0.0004 Å |
| b | 17.0098 ± 0.0005 Å |
| c | 28.8179 ± 0.0008 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 8312.5 ± 0.4 Å3 |
| Cell temperature | 143 ± 2 K |
| Ambient diffraction temperature | 143 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 61 |
| Hermann-Mauguin space group symbol | P b c a |
| Hall space group symbol | -P 2ac 2ab |
| Residual factor for all reflections | 0.0487 |
| Residual factor for significantly intense reflections | 0.0358 |
| Weighted residual factors for significantly intense reflections | 0.0819 |
| Weighted residual factors for all reflections included in the refinement | 0.087 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 287068 (current) | 2023-10-21 | cif/ Adding structures of 7714273, 7714274, 7714275, 7714276, 7714277, 7714278, 7714279, 7714280 via cif-deposit CGI script. |
7714276.cif |
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Users of the data should acknowledge the original authors of the
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