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Information card for entry 7714355
Preview
| Coordinates | 7714355.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C38 H64 Br4 Cl6 O2 Rh2 |
|---|---|
| Calculated formula | C38 H64 Br4 Cl6 O2 Rh2 |
| Title of publication | Rhodium complexes with planar-chiral cyclopentadienyl ligands: synthesis from tert-butylacetylene and catalytic performance in C-H activation of arylhydroxamates |
| Authors of publication | Kolos, Andrey; Nelyubina, Yulia V.; Podyacheva, Evgeniya; Perekalin, Dmitry S. |
| Journal of publication | Dalton Transactions |
| Year of publication | 2023 |
| a | 10.2647 ± 0.0003 Å |
| b | 10.4313 ± 0.0003 Å |
| c | 12.9342 ± 0.0004 Å |
| α | 82.315 ± 0.002° |
| β | 73.935 ± 0.002° |
| γ | 67.629 ± 0.002° |
| Cell volume | 1230.05 ± 0.07 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.046 |
| Residual factor for significantly intense reflections | 0.04 |
| Weighted residual factors for significantly intense reflections | 0.0987 |
| Weighted residual factors for all reflections included in the refinement | 0.1017 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 287184 (current) | 2023-11-01 | cif/ Adding structures of 7714352, 7714353, 7714354, 7714355, 7714356, 7714357, 7714358, 7714359, 7714360, 7714361 via cif-deposit CGI script. |
7714355.cif |
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Users of the data should acknowledge the original authors of the
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