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Information card for entry 7714444
Preview
| Coordinates | 7714444.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | CF3-tBu-POCNP-Ni-Cl |
|---|---|
| Formula | C20 H24 Cl F3 N Ni O P |
| Calculated formula | C20 H24 Cl F3 N Ni O P |
| Title of publication | Structures of nickel chloride and thiolate complexes supported by PCN and POCOP pincer ligands and catalytic reactivity of the chloride complexes |
| Authors of publication | Mao, Jia-Xue; Chang, Jiarui; Zhang, Jie; Chen, Xuenian |
| Journal of publication | Dalton Transactions |
| Year of publication | 2023 |
| a | 14.3139 ± 0.0003 Å |
| b | 10.1907 ± 0.0002 Å |
| c | 15.4819 ± 0.0004 Å |
| α | 90° |
| β | 109.397 ± 0.003° |
| γ | 90° |
| Cell volume | 2130.14 ± 0.09 Å3 |
| Cell temperature | 170 ± 0.1 K |
| Ambient diffraction temperature | 170 ± 0.1 K |
| Number of distinct elements | 8 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0848 |
| Residual factor for significantly intense reflections | 0.0739 |
| Weighted residual factors for significantly intense reflections | 0.2154 |
| Weighted residual factors for all reflections included in the refinement | 0.2242 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.073 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 287500 (current) | 2023-11-10 | cif/ Adding structures of 7714441, 7714442, 7714443, 7714444, 7714445 via cif-deposit CGI script. |
7714444.cif |
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