Crystallography Open Database

Information card for entry 7714599

Preview

Coordinates	7714599.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H Na6 O24 Sb W6
Calculated formula	Na6 O52 Sb W6
Title of publication	Heteroelements in polyoxometalates: a study on the influence of different group 15 elements on polyoxometalate formation.
Authors of publication	Raabe, Jan-Christian; Jameel, Froze; Stein, Matthias; Albert, Jakob; Poller, Maximilian J.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	2
Pages of publication	454 - 466
a	10.5698 ± 0.0005 Å
b	10.977 ± 0.0004 Å
c	11.341 ± 0.0005 Å
α	69.081 ± 0.004°
β	85.409 ± 0.004°
γ	69.784 ± 0.004°
Cell volume	1151.98 ± 0.1 Å³
Cell temperature	99.98 ± 0.1 K
Ambient diffraction temperature	99.98 ± 0.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0259
Residual factor for significantly intense reflections	0.0254
Weighted residual factors for significantly intense reflections	0.0686
Weighted residual factors for all reflections included in the refinement	0.0689
Goodness-of-fit parameter for all reflections included in the refinement	1.136
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
289518 (current)	2024-02-04	cif/ Updating files of 7714599, 7714600, 7714601, 7714602 Original log message: Adding full bibliography for 7714599--7714602.cif.	7714599.cif
288024	2023-12-05	cif/ Adding structures of 7714599, 7714600, 7714601, 7714602 via cif-deposit CGI script.	7714599.cif