Crystallography Open Database

Information card for entry 7714602

Preview

Coordinates	7714602.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	As H5.9 Na3.1 O34 W9
Calculated formula	As K1.35 Na3.15 O47.5 W9
Title of publication	Heteroelements in polyoxometalates: a study on the influence of different group 15 elements on polyoxometalate formation.
Authors of publication	Raabe, Jan-Christian; Jameel, Froze; Stein, Matthias; Albert, Jakob; Poller, Maximilian J.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	2
Pages of publication	454 - 466
a	30.0854 ± 0.00009 Å
b	30.0854 ± 0.00009 Å
c	30.0854 ± 0.00009 Å
α	90°
β	90°
γ	90°
Cell volume	27231.2 ± 0.14 Å³
Cell temperature	99.95 ± 0.13 K
Ambient diffraction temperature	99.95 ± 0.13 K
Number of distinct elements	5
Space group number	229
Hermann-Mauguin space group symbol	I m -3 m
Hall space group symbol	-I 4 2 3
Residual factor for all reflections	0.0585
Residual factor for significantly intense reflections	0.0422
Weighted residual factors for significantly intense reflections	0.0918
Weighted residual factors for all reflections included in the refinement	0.107
Goodness-of-fit parameter for all reflections included in the refinement	1.12
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
289518 (current)	2024-02-04	cif/ Updating files of 7714599, 7714600, 7714601, 7714602 Original log message: Adding full bibliography for 7714599--7714602.cif.	7714602.cif
288024	2023-12-05	cif/ Adding structures of 7714599, 7714600, 7714601, 7714602 via cif-deposit CGI script.	7714602.cif