Crystallography Open Database

Information card for entry 7714810

Preview

Coordinates	7714810.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C234 H388 Cl116 N16 Ni24 O88
Calculated formula	C176 H272 N16 Ni24 O88
Title of publication	Tetracosanuclear nickel complexes as effective catalysts for cycloaddition of carbon dioxide with epoxides.
Authors of publication	Liu, Guan-Lin; Wu, En-Hsu; Hung, Yu-Ching; Chou, Wei-Chi; Hung, Chia-Hsin; Lin, Chu-Chieh; Ko, Bao-Tsan
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	4
Pages of publication	1425 - 1429
a	24.885 ± 0.0012 Å
b	24.885 ± 0.0012 Å
c	73.876 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	45749 ± 5 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.0963
Residual factor for significantly intense reflections	0.0846
Weighted residual factors for significantly intense reflections	0.2303
Weighted residual factors for all reflections included in the refinement	0.2375
Goodness-of-fit parameter for all reflections included in the refinement	1.128
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
289505 (current)	2024-02-04	cif/ Updating files of 7714805, 7714806, 7714807, 7714808, 7714809, 7714810 Original log message: Adding full bibliography for 7714805--7714810.cif.	7714810.cif
288494	2023-12-22	cif/ Adding structures of 7714805, 7714806, 7714807, 7714808, 7714809, 7714810 via cif-deposit CGI script.	7714810.cif