Crystallography Open Database

Information card for entry 7715371

Preview

Coordinates	7715371.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H23 Al N2
Calculated formula	C23 H23 Al N2
SMILES	[Al]1([n]2c(C(N1C=C1c3c(c4c1cccc4)cccc3)C)cccc2)(C)C
Title of publication	Novel bidentate <i>N</i>-coordinated alkylaluminum complexes: synthesis, characterization, and efficient catalysis for hydrophosphonylation.
Authors of publication	Wei, Biao; Wang, Chaoqun; Miao, Hui; Qin, Zhibiao; Huang, Mengna; Xu, Yan; Xue, Wenhui; Yang, Shucheng; Liu, Chenxu; Bai, Cuibing; Chen, Zheng
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	9
Pages of publication	4185 - 4193
a	16.7984 ± 0.0009 Å
b	11.7252 ± 0.0005 Å
c	20.9895 ± 0.0009 Å
α	90°
β	104.505 ± 0.005°
γ	90°
Cell volume	4002.4 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	I 1 2/a 1
Hall space group symbol	-I 2ya
Residual factor for all reflections	0.1131
Residual factor for significantly intense reflections	0.0579
Weighted residual factors for significantly intense reflections	0.151
Weighted residual factors for all reflections included in the refinement	0.1775
Goodness-of-fit parameter for all reflections included in the refinement	0.972
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
290063 (current)	2024-03-04	cif/ Adding structures of 7715369, 7715370, 7715371, 7715372, 7715373 via cif-deposit CGI script.	7715371.cif