Crystallography Open Database

Information card for entry 7715561

Preview

Coordinates	7715561.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H48 Cr N4 P4
Calculated formula	C20 H48 Cr N4 P4
Title of publication	Catalytic dinitrogen reduction to hydrazine and ammonia using Cr(N<sub>2</sub>)<sub>2</sub>(diphosphine)<sub>2</sub> complexes.
Authors of publication	Beasley, Charles H.; Duletski, Olivia L.; Stankevich, Ksenia S.; Arulsamy, Navamoney; Mock, Michael T.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	15
Pages of publication	6496 - 6500
a	8.2082 ± 0.0004 Å
b	10.3281 ± 0.0005 Å
c	16.6727 ± 0.0008 Å
α	104.253 ± 0.002°
β	90.264 ± 0.002°
γ	102.507 ± 0.002°
Cell volume	1334.9 ± 0.11 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0346
Residual factor for significantly intense reflections	0.029
Weighted residual factors for significantly intense reflections	0.0696
Weighted residual factors for all reflections included in the refinement	0.0736
Goodness-of-fit parameter for all reflections included in the refinement	1.084
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
291656 (current)	2024-05-05	cif/ Updating files of 7715561, 7715562 Original log message: Adding full bibliography for 7715561--7715562.cif.	7715561.cif
290665	2024-03-27	cif/ Adding structures of 7715561, 7715562 via cif-deposit CGI script.	7715561.cif