Crystallography Open Database

Information card for entry 7715773

Preview

Coordinates	7715773.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H22 B N
Calculated formula	C14 H22 B N
Title of publication	Bidentate Boron Lewis Acids: Synthesis by Tin Boron Exchange Reaction and Host-Guest Complex Formation
Authors of publication	Beckmann, Jean Louis; Neumann, Beate; Stammler, Georg; Lamm, Jan-Hendrik; Mitzel, Norbert Werner
Journal of publication	Dalton Transactions
Year of publication	2024
a	14.22709 ± 0.00018 Å
b	15.98244 ± 0.00015 Å
c	23.7578 ± 0.0002 Å
α	90°
β	100.083 ± 0.0011°
γ	90°
Cell volume	5318.7 ± 0.1 Å³
Cell temperature	99.94 ± 0.15 K
Ambient diffraction temperature	99.94 ± 0.15 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	I 1 2/a 1
Hall space group symbol	-I 2ya
Residual factor for all reflections	0.0404
Residual factor for significantly intense reflections	0.0362
Weighted residual factors for significantly intense reflections	0.0903
Weighted residual factors for all reflections included in the refinement	0.0942
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
291268 (current)	2024-04-18	cif/ Adding structures of 7715770, 7715771, 7715772, 7715773, 7715774, 7715775, 7715776, 7715777, 7715778, 7715779, 7715780, 7715781 via cif-deposit CGI script.	7715773.cif