Crystallography Open Database

Information card for entry 7716396

Preview

Coordinates	7716396.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H33 F12 Ge N O2
Calculated formula	C34 H33 F12 Ge N O2
Title of publication	Synthesis, structure, and alkynylation reactivity of alkynyl-silicate, -germanate, and -stannate.
Authors of publication	Iwabuchi, Shuta; Morofuji, Tatsuya; Kano, Naokazu
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	26
Pages of publication	10829 - 10833
a	11.1071 ± 0.0005 Å
b	16.2492 ± 0.0009 Å
c	18.3357 ± 0.0008 Å
α	90°
β	95.828 ± 0.004°
γ	90°
Cell volume	3292.1 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0673
Residual factor for significantly intense reflections	0.0436
Weighted residual factors for significantly intense reflections	0.0759
Weighted residual factors for all reflections included in the refinement	0.0819
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
293042 (current)	2024-07-05	cif/ Updating files of 7716394, 7716395, 7716396 Original log message: Adding full bibliography for 7716394--7716396.cif.	7716396.cif
292482	2024-06-21	cif/ Adding structures of 7716394, 7716395, 7716396 via cif-deposit CGI script.	7716396.cif