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Information card for entry 7716908
Preview
| Coordinates | 7716908.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23 H32 N3 Ni O2 P S2 |
|---|---|
| Calculated formula | C23 H32 N3 Ni O2 P S2 |
| Title of publication | Synthesis and reactivity of air stable Ni(II) complexes with isocyanides and dialkyldithiophosphate ligands: acyclic diaminocarbene formation. |
| Authors of publication | Álvarez-Miguel, Lucía; Del Carmen-Rodríguez, Clara; Valle, María; Álvarez, Celedonio M; Martín-Álvarez, José M; García-Rodríguez, Raúl; Miguel, Daniel |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2024 |
| Journal volume | 53 |
| Journal issue | 36 |
| Pages of publication | 15101 - 15112 |
| a | 14.1712 ± 0.0003 Å |
| b | 14.4321 ± 0.0004 Å |
| c | 14.8981 ± 0.0003 Å |
| α | 90° |
| β | 100.956 ± 0.002° |
| γ | 90° |
| Cell volume | 2991.43 ± 0.12 Å3 |
| Cell temperature | 293 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0559 |
| Residual factor for significantly intense reflections | 0.0367 |
| Weighted residual factors for significantly intense reflections | 0.0855 |
| Weighted residual factors for all reflections included in the refinement | 0.0954 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 295256 (current) | 2024-10-06 | cif/ Updating files of 7716902, 7716903, 7716904, 7716905, 7716906, 7716907, 7716908, 7716909, 7716910, 7716911, 7716912, 7716913, 7716914, 7716915, 7716916, 7716917, 7716918 Original log message: Adding full bibliography for 7716902--7716918.cif. |
7716908.cif |
| 294257 | 2024-08-29 | cif/ Adding structures of 7716902, 7716903, 7716904, 7716905, 7716906, 7716907, 7716908, 7716909, 7716910, 7716911, 7716912, 7716913, 7716914, 7716915, 7716916, 7716917, 7716918 via cif-deposit CGI script. |
7716908.cif |
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Users of the data should acknowledge the original authors of the
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