Crystallography Open Database

Information card for entry 7717004

Preview

Coordinates	7717004.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H68 Cl3 Co N4 P2 Si2
Calculated formula	C38 H68 Cl3 Co N4 P2 Si2
Title of publication	Dinitrogen silylation catalyzed by silylene cobalt(I) and silylene iron(I) chlorides.
Authors of publication	Fan, Qingqing; Li, Qingshuang; Sun, Hongjian; Li, Xiaoyan
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	39
Pages of publication	16261 - 16270
a	13.654 ± 0.0001 Å
b	20.1812 ± 0.0002 Å
c	16.8073 ± 0.0002 Å
α	90°
β	92.5 ± 0.001°
γ	90°
Cell volume	4626.91 ± 0.08 Å³
Cell temperature	173 ± 0.1 K
Ambient diffraction temperature	173.15 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0565
Residual factor for significantly intense reflections	0.048
Weighted residual factors for significantly intense reflections	0.1273
Weighted residual factors for all reflections included in the refinement	0.1316
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
296553 (current)	2024-12-06	cif/ Updating files of 7717003, 7717004, 7717005, 7717006 Original log message: Adding full bibliography for 7717003--7717006.cif.	7717004.cif
294749	2024-09-14	cif/ Adding structures of 7717003, 7717004, 7717005, 7717006 via cif-deposit CGI script.	7717004.cif