Crystallography Open Database

Information card for entry 7717283

Preview

Coordinates	7717283.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H24 Br Cu N2 O
Calculated formula	C21 H24 Br Cu N2 O
Title of publication	Exploring the reductive CO<sub>2</sub> fixation with amines and hydrosilanes using readily available Cu(II) NHC-phenolate catalyst precursors.
Authors of publication	Meloni, Giammarco; Morgan, Luca; Cappelletti, David; Bevilacqua, Matteo; Graiff, Claudia; Pinter, Piermaria; Biffis, Andrea; Tubaro, Cristina; Baron, Marco
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	45
Pages of publication	18128 - 18140
a	15.9866 ± 0.0003 Å
b	12.915 ± 0.0003 Å
c	10.0896 ± 0.0002 Å
α	90°
β	91.323 ± 0.002°
γ	90°
Cell volume	2082.61 ± 0.07 Å³
Cell temperature	301 ± 2 K
Ambient diffraction temperature	301 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0404
Residual factor for significantly intense reflections	0.0386
Weighted residual factors for significantly intense reflections	0.1158
Weighted residual factors for all reflections included in the refinement	0.1189
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
296602 (current)	2024-12-06	cif/ Updating files of 7717282, 7717283 Original log message: Adding full bibliography for 7717282--7717283.cif.	7717283.cif
295598	2024-10-24	cif/ Adding structures of 7717282, 7717283 via cif-deposit CGI script.	7717283.cif