Crystallography Open Database

Information card for entry 7717500

Preview

Coordinates	7717500.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H38 Cl3 N3 Ni O3 P2
Calculated formula	C25 H38 Cl3 N3 Ni O3 P2
Title of publication	Simple and easy functionalization of <i>para</i>-hydroxy POCOP-M (M = Ni(II), Pd(II)) pincer complexes: synthesis of multimetallic species.
Authors of publication	Serrano-García, Juan S; García-Eleno, Marco Antonio; Arenaza-Corona, Antonino; Rufino-Felipe, Ernesto; Valdés, Hugo; Hernandez-Ortega, Simon; Morales-Morales, David
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	2
Pages of publication	694 - 699
a	8.0717 ± 0.0009 Å
b	28.421 ± 0.003 Å
c	13.667 ± 0.0014 Å
α	90°
β	94.878 ± 0.002°
γ	90°
Cell volume	3123.9 ± 0.6 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0842
Residual factor for significantly intense reflections	0.0444
Weighted residual factors for significantly intense reflections	0.0661
Weighted residual factors for all reflections included in the refinement	0.0734
Goodness-of-fit parameter for all reflections included in the refinement	0.806
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
298880 (current)	2025-04-05	cif/ Updating files of 7717499, 7717500, 7717501, 7717502 Original log message: Adding full bibliography for 7717499--7717502.cif.	7717500.cif
295922	2024-11-15	cif/ Adding structures of 7717499, 7717500, 7717501, 7717502 via cif-deposit CGI script.	7717500.cif