Crystallography Open Database

Information card for entry 7717739

Preview

Coordinates	7717739.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H61 Ge K N2 O6 Si3
Calculated formula	C32 H61 Ge K N2 O6 Si3
Title of publication	Synthesis and exploration of a 1<i>H</i>-germol-1-ide/pyridine bidentate ligand.
Authors of publication	Liu, Chenghuan; Schmidtmann, Marc; Müller, Thomas
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	5
Pages of publication	2005 - 2010
a	19.6032 ± 0.0009 Å
b	10.9806 ± 0.0005 Å
c	20.4878 ± 0.0008 Å
α	90°
β	110.145 ± 0.0014°
γ	90°
Cell volume	4140.3 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0546
Residual factor for significantly intense reflections	0.041
Weighted residual factors for significantly intense reflections	0.0817
Weighted residual factors for all reflections included in the refinement	0.0867
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
298266 (current)	2025-03-04	cif/ Updating files of 7717739, 7717740, 7717741, 7717742 Original log message: Adding full bibliography for 7717739--7717742.cif.	7717739.cif
297012	2025-01-01	cif/ Adding structures of 7717739, 7717740, 7717741, 7717742 via cif-deposit CGI script.	7717739.cif