Crystallography Open Database

Information card for entry 7717746

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Coordinates	7717746.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H17 P Si
Calculated formula	C18 H17 P Si
Title of publication	Phosphorus-containing polycarbosilazanes: synthesis <i>via</i> dehydrocoupling catalysis and flame-retardant properties.
Authors of publication	Soran, Albert; Chapple, Peter M.; Longuet, Claire; Sonnier, Rodolphe; Cordier, Marie; Carpentier, Jean-François; Sarazin, Yann
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	5
Pages of publication	2037 - 2054
a	10.8294 ± 0.0009 Å
b	8.7426 ± 0.0007 Å
c	16.9192 ± 0.001 Å
α	90°
β	91.869 ± 0.003°
γ	90°
Cell volume	1601 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0242
Residual factor for significantly intense reflections	0.0213
Weighted residual factors for significantly intense reflections	0.0541
Weighted residual factors for all reflections included in the refinement	0.056
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
298270 (current)	2025-03-04	cif/ Updating files of 7717745, 7717746 Original log message: Adding full bibliography for 7717745--7717746.cif.	7717746.cif
297014	2025-01-01	cif/ Adding structures of 7717745, 7717746 via cif-deposit CGI script.	7717746.cif