Crystallography Open Database

Information card for entry 7719301

7719300 << 7719301 >> 7719302

Preview

Coordinates	7719301.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C168 H288 F36 Ge84 N68 O176
Calculated formula	C168 H288.005 F36 Ge84 N68 O176
Title of publication	Structure-directing synthesis of two germanate cages featuring odd-member ring windows.
Authors of publication	Li, Hao; Xu, Yanan; Zhang, Shiyue; Gu, Pengliang; Hu, Qing; Zhang, Yu; Wang, Wenkai; Shi, Zhan; Fu, Xinyi; Du, Hongbin
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	36
Pages of publication	13775 - 13782
a	24.0248 ± 0.0006 Å
b	24.0248 ± 0.0006 Å
c	35.81 ± 0.0012 Å
α	90°
β	90°
γ	90°
Cell volume	20669.2 ± 1 Å³
Cell temperature	299 K
Ambient diffraction temperature	299 K
Number of distinct elements	6
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.0573
Residual factor for significantly intense reflections	0.0521
Weighted residual factors for significantly intense reflections	0.1398
Weighted residual factors for all reflections included in the refinement	0.143
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
302645 (current)	2025-10-06	cif/ Updating files of 7719300, 7719301 Original log message: Adding full bibliography for 7719300--7719301.cif.	7719301.cif
301876	2025-08-23	cif/ Adding structures of 7719300, 7719301 via cif-deposit CGI script.	7719301.cif