Crystallography Open Database

Information card for entry 7719838

7719837 << 7719838 >> 7719839

Preview

Coordinates	7719838.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H22 B10 Cl2
Calculated formula	C18 H22 B10 Cl2
Title of publication	Nickel-catalyzed 1,2-dialkenylation of <i>o</i>-carboranes with alkenyl bromides.
Authors of publication	Zhuo, Qihang; Zhang, Jie; Xie, Zuowei
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	47
Pages of publication	17430 - 17433
a	7.286 ± 0.007 Å
b	12.443 ± 0.009 Å
c	12.891 ± 0.011 Å
α	84.61 ± 0.03°
β	77.99 ± 0.03°
γ	82.09 ± 0.03°
Cell volume	1129.7 ± 1.7 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0881
Residual factor for significantly intense reflections	0.0613
Weighted residual factors for significantly intense reflections	0.1441
Weighted residual factors for all reflections included in the refinement	0.1595
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
304103 (current)	2025-12-07	cif/ Updating files of 7719835, 7719836, 7719837, 7719838, 7719839, 7719840 Original log message: Adding full bibliography for 7719835--7719840.cif.	7719838.cif
303219	2025-11-07	cif/ Adding structures of 7719835, 7719836, 7719837, 7719838, 7719839, 7719840 via cif-deposit CGI script.	7719838.cif